Metal-Ion Separation and Preconcentration: Progress and by Andrew H. Bond, Mark L. Dietz, Robin D. Rogers

By Andrew H. Bond, Mark L. Dietz, Robin D. Rogers

Steel ion separation and preconcentration represent the pivotal step in different analytical, purification, and waste remedy methods. expanding environmental laws and transforming into monetary incentives indicate that separation technological know-how could be necessary to the way forward for business processing. This quantity deals a vast viewpoint of advances within the box whereas additionally together with up to date paintings in a few really good components. It starts with an outline which describes the targets the ebook, summarizes each one bankruptcy, and offers a few rapid demanding situations for the long run. evaluation chapters then deal with the prestige of steel ion separations in nuclear power and defense-related courses. those are via twenty chapters masking a variety of issues, together with aqueous stages in separations, extractant layout and synthesis, solvent extraction, solid-liquid distribution, separations utilizing membranes, centrifugal partition and countercurrent chromatography, and supercritical fluid extraction platforms. jointly the essays offer a great stability of basic and utilized examine, making the e-book useful for either amateur and skilled practitioners.

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Extra resources for Metal-Ion Separation and Preconcentration: Progress and Opportunities (ACS Symposium Series)

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4 M TBP-ra-dodecane. 5 χ 10 , which allowed disposal of the process raffinâtes as low-level wastes. Approximately 18 g of U, 84 g of Pu and 200 mg of Am were recovered. s achieved, several other features of these processing runs are noteworthy. 9% of the Am. An innovative scrub/Am strip section was designed and tested to reduce the number of stages required for stripping and at the same time to concentrate Am by a factor of -17. 28 Μ (NH4)2C204 solution was used to strip Pu and prevent its precipitation.

The GTM is composed of four major sections: (1) SASSE (Spreadsheet Algorithm for Stagewise Solvent Extraction), (2) SASPE (Spreadsheet Algorithm for Speciation and Partitioning Equilibria), (3) SPACE (Size of Plant and Cost Estimates) and (4) INPUT/OUTPUT. All four sections interact together and are executed by Microsoft Excel software. SASSE calculates multistage, countercurrentflowsheetsbased on distribution ratios calculated in the SASPE section. SPACE enables one to estimate the space and cost requirements for installing a specific TRUEX process using a variety of different equipment and processing facilities.

Depending on the composition of the streams, oxalic acid is sometimes added to suppress the extraction of Fe, Zr, Mo and Pd. Reducing agents, such as ferrous sulfamate, may be added to ensure that neptunium is in the tetravalent oxidation state. 03 M H2C2O4, but if an unusually high concentration of Zr is present in the feed, different scrubbing regimes may be required. 05 M HF or ammonium oxalate to solubilize macroquantities of Pu. Uranyl ion and pertechnetate are removed from the process solvent during solvent washing with dilute carbonate solution.

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