Miniaturization and Mass Spectrometry, 1st Edition by Séverine Gac, Albert Berg

By Séverine Gac, Albert Berg

The explosion within the past due twentieth century of the sphere of analytical chemistry and especially for organic reasons has ended in a necessity for quick, built-in, moveable, extra trustworthy and extra delicate instruments which may deal with diminished volume of samples. Microfluidics and lab-on-a-chip units supply a great solution to this quest to miniaturized and improved research they usually lend themselves good to mass spectrometric detection as related quantities of samples within the low microliter variety are dealt with on a chip and required for a unmarried MS research.

Miniaturization and Mass Spectrometry illustrates this pattern and specializes in one specific research strategy, mass spectrometry whose reputation has "dramatically" elevated within the final twenty years with the explosion of the sector of organic research and the advance of 2 "soft" ionization suggestions, ESI and MALDI which allow the research of enormous yet fragile molecules, corresponding to organic molecules (DNA, proteins, oligosaccharides).

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The inset shows the cross-section of the capillary with the main channel viewed from the bottom. d. d. d. Teflon sleeve to the edge of the device. d. d. was inserted into the first one until it made contact with the device. Finally, the capillary was inserted into the inner Teflon sleeve until it cleanly aligned with the etched channel of the microfabricated device. The whole assembly was held in place and was stabilized by a Teflon tube dual-shrink placed on top of the two Teflon sleeves. The alignment of this interface was critical and very time consuming.

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